Get Analysis of the New Metals. Titanium, Zirconium, Hafnium, PDF

By W. T. Elwell

ISBN-10: 0080118038

ISBN-13: 9780080118031

Publication by means of Elwell, W T wooden, D F

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Additional resources for Analysis of the New Metals. Titanium, Zirconium, Hafnium, Niobium, Tantalum, Tungsten and Their Alloys

Sample text

Platinum-black may be displaced from the electrode surfaces if the electrodes are removed frequently. (3) If the cell factor changes significantly (say, outside ±0-005), the 50-g counterpoise may be adjusted so as to alter the volume of solution used, thereby maintaining a reasonably constant factor. The cell counterpoise may also be adjusted if any alteration is made which affects the cell weight. (4) Supplied by Imperial Chemical Industries Limited. The volume of "Lissapol" N solution required is best found by trial, and usually varies from 1 to 5 drops.

Dissolve 0-5657 g of potassium dichromate (dried at 140-150°C) in water and dilute to 1 1. Dilute 100 ml of this solution to 1 1. 2. Preparation of Calibration Graph (Note) Transfer 40 ml of sulphuric acid ( 1 + 4 ) to each of six conical beakers (250ml) and add, separately, 5 0 , 1 0 0 , 1 5 0 , 2 0 0 and 2 5 0 m l of the standard chromium solution (1 ml = 0 0 2 m g Cr). U s e the remaining solution as a blank. ). Evaporate the solution until fumes of sulphuric acid are just evolved, then cool and dilute to 70 ml.

2. 1. Special Procedure Reagents EDTA Solution (0-75%). Dissolve 3-75 g of the disodium dihydrate salt of ethylenediaminetetra-acetic acid (EDTA) in water and dilute to 500 ml. 1. 2. Preparation 5-100 ppm of Calibration Graph—for Copper Contents Transfer 0-5 g of high-purity titanium to each of six beakers, and dissolve the metal in 25 ml of sulphuric acid (1 + 4 ) and 0-5 ml of fluoroboric acid; warm gently to assist solution. Oxidize each solution with a slight excess of cone, nitric acid, added dropwise, and boil gently to expel oxides of nitrogen.

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Analysis of the New Metals. Titanium, Zirconium, Hafnium, Niobium, Tantalum, Tungsten and Their Alloys by W. T. Elwell


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